TESTING THE INTEGRITY OF GLOVEBOX
GLOVES FOR SUB-VIRAL SIZE DEFECTS
UTILIZING ELECTRON BEAMS
Gregory J. Gormley
ConverTec Corporation
AGS Annual Conference 2000
Hotel Inter-Continental
New Orleans, Louisiana
August 23, 2000
Introduction: The Problem !
"….weakest link in the containment barrier".
"….the Achilles’ Heal".
Challenge: Resolve The Issue !
Solution: Integrity Testing Utilizing Electron
Beam Technology
Technology Application in Glove Manufacturing
Technology Application With-in Glovebox
Technology Application Out-side Glovebox
Water Leak
Test (Fill the Product with Water)
Electrical
Hydraulic Test (Submerge the Product in Water)
Limitations:
Conformal Electrode Mandrel, Wet Test, Electrical Potential Applied, Short Circuit Indicator, Large Straight Holes Only (50 Microns Plus), No Anomalies, Water Surface Tension, Product Dried with Hot Air (Ozone)
Dry Test
or Spark Test (Electrically Charged Brush)
Limitations:
Direct Contact, 1.3 to 1.5 kV AC @ 60 Hz, Conformal Electrode Mandrel, Large Destructive Spark, Large Straight Holes Only (50 to 100 Microns Plus).
Capacitive
Test (Submerge the Product in Water)
Limitations:
Conformal Electrode Mandrel, Wet Test, Different Frequencies (Not Just DC or 60 Hz), Discovery of Holes, Blisters, and Bubbles, Repeatability and Calibration Difficult, Integral Measurement (Gray or Average Measurement), Product Dried with Hot Air (Ozone).
Statistical
Testing (Destructive Test)
Limitations:
Sample Finished Production, Product is Destroyed in Process, Not 100% Tested, Mathematical Prediction, Implied AQL Level with Acceptable "Rejects".
Oxygen
Leak Test (Non-Destructive Test)
Limitations:
Expensive, Limited to the Hand and FingerTips, Cumbersome, Uncomfortable Working Design, Time Consuming.
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Electron Beam Technology: (Corona Beam or C-Beam)
Advantages:
Dry Test
Product Tested on Molding Mandrel (Providing
Curing Is Not Required)In-Line in Real-Time
Non-Contact
Based On Point-To-Point Effect
Griebel-Gormley Aperture Effect (Anomaly Acts as a "Point")
Cover Gas Creates a "Focal Area" (nitrogen)
C-Beam Self Seeking in Focal Area
C-Beam Follows a Tortuous Path
C-Beam Articulates to Find Its’ Potential
Finds "ALL ANOMALIES" (Sub-Viral Size Holes and Voids, Bubbles, Blisters, Contamination, Stress Fractures, Formulation Defects, Low Density Areas, Uncatalyzed or Unblended Resin, etc.)
Discrete Measurement (No Average)
Measures Electric Discharge (Volume of Electrons)
Constructive and Destructive Interference (Frequency Changes at Sensor)
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C-Beam Applications: (Three Methodologies)
1ST . At Glove Manufacturing Facility
In-Line with the Manufacturing Process
(No Labor Cost with Handling)Testing is Final Step before Unloading
2nd . Test Within the GloveboxC-Beam Sensor is Located Inside the Glovebox above the Glove Port in Reach of Operator3rd . Test Outside of the Glovebox With the GloveMultiple Sensors at Each Port Location-Test At Will
Inside-Out With a Hand-held Sensor Gun
Conclusion:
Glovebox Integrity Does Not Have To Be Compromised If C-Beam Technology Is Implemented and EVERYONE PLAYS THEIR PART.
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